收稿日期: 2017-05-17
修回日期: 2017-12-25
网络出版日期: 2018-05-19
Optimum Condition Selection of Determining Trace Gold by Bubble Plastic Adsorption-Graphite Furnace Atomic Absorption Spectrometry Method Un-der the Environment of Low Oxygen and Low Pressure
Received date: 2017-05-17
Revised date: 2017-12-25
Online published: 2018-05-19
关键词: 低氧低分压环境; 痕量金测定; 富集分离; 泡塑吸附—石墨炉原子吸收光谱法; 高海拔地区
聂凤莲 , 张浥宁 , 王立华 . 低氧低分压环境下泡塑吸附—石墨炉原子吸收光谱法测定痕量金的最佳条件选择[J]. 黄金科学技术, 2018 , 26(2) : 234 -240 . DOI: 10.11872/j.issn.1005-2518.2018.02.234
[1] 薛光.金的分析化学[M].北京:宇航出版社,1990:94-591.
Xue Guang.Analytical Chemistry of Gold[M].Beijing:Astronautic Publishing House,1990:94-591.
[2] 李占江.金银及有色金属地勘矿冶分析手册[M].北京:地质出版社,2013:28-262.
Li Zhanjiang.Handbook of Analysis of Gold and Silver and Nonferrous Metals[M].Beijing:Geological Publishing House,2013:28-262.
[3] 李小红,储溱,张蕾,等.泡沫塑料富集—电感耦合等离子体质谱法测定地球样品中痕量金 [J]资源环境与工程,2006,20(3):329-331.
Li Xiaohong,Chu Qin,Zhang Lei,et al.Measuration of trace gold in geological samples by goam-in ductively coupled plasma mass spectrometry method[J]Resources Environment and Engineering,2006,20(3):329-331.
[4] 李锟.聚氨酯泡沫塑料富集——ICP-MS 测定化探样中微量金的方法[J].化工矿产地质,2007,29(4):242-244.
Li Kun.Enrichment of polyaminoester foamed plastics measure to determine the trace Au by ICP-MS[J].Geology of Chemical Minerals,2007,29(4):242-244.
[5] 张勇,王玉功,刘建军.封闭溶样—电感耦合等离子体质谱法测定地质样品中痕量金[J].中国无机分析化学,2013,3(1):34-37.
Zhang Yong,Wang Yugong,Liu Jianjun.Determination of trace gold in geological samples by inductively coupled plasma mass spectrometry with pressurized sample decomposition technique[J].Chinese Journal of Inorganic Analytical Chemistry,2013,3(1):34-37.
[6] 孙晓玲,于照水,张勤.泡沫塑料吸附富集—石墨炉原子吸收光谱法测定勘查地球化学样品中超痕量金[J].岩矿测试,2002,21(4):266-269.
Sun Xiaoling,Yu Zhaoshui,Zhang Qin.Determination of ultra-trace gold in geochemical exploration samples by GFAAS after preconcentration with polyurethane foam[J].Rock and Mineral Analysis,2002,21(4):266-269.
[7] 张碧玲,孙爱琴,姚文生,等.石墨炉原子吸收测定岩石样品中痕量金的研究[J].黄金,2005,26(5):42-44.
Zhang Biling,Sun Aiqin,Yao Wensheng,et al.Research on trace gold determination in rock samples using graphite oven atomic absorption method[J].Gold,2005,26(5):42-44.
[8] 艾晓军,鞠军.泡沫塑料富集分离金中几个问题的探讨[J].黄金,2008,29(2):46-49.
Ai Xiaojun,Ju Jun.Research on several problems in enrichment and separation of gold with foam plastic[J].Gold,2008,29(2):46-49.
[9] 宋丽华,金一.石墨炉原子吸收光谱法测定化探样品中痕量金[J].理化检验—化学分册,2009,45(6):692 -694.
Song Lihua,Jin Yi.GFAAS determination of trace amount of gold in geochemical exploration sample[J].Physical Testing and Analysis Part B:Chemical Analysis,2009,45(6):692-694.
[10] 艾晓军,聂凤莲,陈雪,等.Z-5000石墨炉原子吸收光谱法测定痕量金检出限的探讨[J].黄金科学技术,2011,19(4):65-67.
Ai Xiaojun,Nie Fenglian,Chen Xue,et al.Study on detection limit of determination of trace gold by Z-5000 graphite furnace atomic absorption spectrometry[J].Gold Science and Technology,2011,19(4):65-67.
[11] 王頔,汪君.泡塑吸附—石墨炉原子吸收光谱法测定勘查地球化学样品中痕量金[J].新疆师范大学学报(自然科学版),2014,33(2):27-31.
Wang Di,Wang Jun.Determination of trace gold in geochemical exploration samples by GFAAS after preconcentration with polyurethane foam[J].Journal of Xinjiang Normal University(Natural Sciences Edition),2014,33(2):27-31.
[12] 王祝,邵蓓,邬国栋,等.低氧低分压环境下泡塑吸附—石墨炉原子吸收光谱法测定化探样品中的痕量金[J].岩矿测试,2010,29(3):282-286.
Wang Zhu,Shao Bei,Wu Guodong,et al.Determination of trace gold in geochemical samples by graphite furnace atomic absorption spectrometry with polyurethane foam preconcentration under hypobaric hypoxia condition[J].Rock and Mineral Analysis,2010,29(3):282-286.
[13] 王培艳,马成冰.低氧低分压环境下泡塑吸附原子吸收光谱法测定矿中的金[J].光谱实验室,2012,29(2) :938-940.
Wang Peiyan,Ma Chengbing.Determination of gold in ore by atomic absorption spectrometry with polyurethane foam absorption under hypobaric hypoxia condition[J].Chinese Journal of Spectoscopy Laboratory,2012,29(2):938-940.
[14] 艾晓军,聂凤莲.Z-5000石墨炉原子吸收光谱法测定痕量金升温程序研究[J].黄金,2006,27(9):42-45.
Ai Xiaojun,Nie Fenglian.Study on the heating procedure for a tomic absorption spectrum method with Z-5000 graphite furnace to measure trace gold[J].Gold,2006,27(9):42-45.
[15] 李勇.Z-2000偏振塞曼石墨炉原子吸收分光光度计测定地球化学样品中痕量金[J].岩矿测试,2008,27(4):305-309.
Li Yong.Determination of trace gold in geochemical exploration samples by Z-2000 polarized zeeman graphite furnace atomic absorption spectrophotometry[J].Rock and Mineral Analysis,2008,27(4):305-309.
[16] 艾晓军,杨理勤,冯亮,等.泡沫塑料吸附—石墨炉测定痕量金方法的改进[J].黄金科学技术,2011,19(5):51-52.
Ai Xiaojun,Yang Liqin,Feng Liang,et al.Method improvement of trace gold determination with the foam plastic adsorption-graphite furnace[J].Gold Science and Technology,2011,19(5):51-52.
[17] 薛光,张汝生,姚万林,等.用微波封闭溶样氢醌滴定法快速测定矿石中金[J].黄金地质,2003,9(3):69-71.
Xue Guang,Zhang Rusheng,Yao Wanlin,et al.The microwave sealing sample hydroquinone titration method for quick determination of gold[J].Gold Geology,2003,9(3):69-71.
[18] 薛光,梁志伟.微波封闭溶样快速测定矿石中金[J].理化检验—化学分册,2005,41(1):50-51.
Xue Guang,Liang Zhiwei.Application of sample dissolution by microwave heating in closed vesseltothe photometrice determination of gold in ores[J].Physical Testing and Analysis Part B:Chemical Analysis,2005,41(1):50-51.
[19] 中华人民共和国国土资源部.地质矿产实验室测试质量管理规范:DZ/T0130-2006[S].北京:中国标准出版社,2006.
Ministry of Land and Resources of the People’s Republic of China.The Specification of testing quality management for geological laboratories:DZ/T0130-2006[S].Beijing:China Standard Publishing House,200
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